In , Emap bought Metro Radio Group and at the start of , Emap decided to scrap Great North Radio and replaced it with local stations under the brand name of Magic , with a new format of Hot Adult Contemporary music. Magic launched on 19 February Tom Davies was the first ever voice heard on Magic and successfully hosted the breakfast show on the station for a number of years. In December , EMAP decided that it was more economical for the Magic network to share off-peak programmes and in line with the other Magic AM stations began networking between 10am-2pm, and 7pm-6am. During these hours it was simply known as Magic , although there were local commercial breaks, and local news on the hour. In January after a decline in listening, [ citation needed ] the station ceased networking with the London station, Magic During networked hours, local adverts are aired, as well as a local news summary on the hour together with local traffic and travel in the afternoon. From July , more networking was introduced across the Northern Magic AM network with only the weekday breakfast with a running length of four hours presented from local studios.
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A for the reporting requirements for federal entities’ audited financial statements. Additional information can be found on the GTAS website. All federal entities must provide Fiscal Service with the required fiscal year-end data that is used to prepare the FR. Reclassified financial statements represent the government-wide financial statement format. Fiscal Service will send a data call to the 40 significant entities, and select other entities, requesting that the CFO of each federal entity designate the certifying officials for various required year-end functions.
Fiscal Service compiles the information from the GTAS submissions for all federal entities into the government-wide financial statements.
Treasury issues bills at a discount with a maturity date of 6 months or less from In accordance with Treasury Financial Manual (TFM)
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Pub Date: , DOI: /chem iridium complexes: (ppy-tfm)2Ir(pico) (Ir1), (dFppy- tfm)2Ir(pico) (Ir2), and.
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It is known to obtain 4-TFMNBA by the steps of first converting 4trifluoromdthylnitroaniline into 4trifluoromethylnitrobenzonitrile by Sandmeyer reaction and then hydrolyzing the nitrile Chem. The product of this process is fairly high in purity as indicated by the reported melting point of However, this process is not suitable for industrial practice because of involving problems such as difficulty of industrially preparing the starting material, 4- trifluoromethylnitroaniline, use of a very toxic cyanide in the essential Sandmeyer reaction and complicatedness of the operations.
However, the product of this method must be low in purity since the reported melting point of the reaction product, 0 C, differs considerably from the aforemetioned melting point. It is an object of the present invention to provide an advantageous and industrially practicable method for preparing 4-TFMNBA. Accordingly both 4-TFMNBA and 4-TFMNBA serve as intermediate materials for synthesizing various fluorine-containing aromatic compounds including ones useful as medicines, agricultural chemicals or liquid crystals.
The starting material for the method according to the invention, a benzotrifluoride derivative of the general formula 1 , is readily available as an industrial material. By nitrating the starting compound with nitric acid or a mixed acid of nitric acid and sulfuric acid the radical Z of the starting compound is simultaneously hydrolyzed into carboxylic group. That is, the aimed nitro-compounds are formed very easily. Accordingly the method of the invention is very suitable and favorable for industrial application.
In the practice of the present invention the nitrating agent is concentrated nitric acid or fuming nitric acid, or a mixed acid of concentrated or fuming nitric acid and concentrated sulfuric acid or fuming sulfuric acid. It is suitable to use 0. The reaction to nitrate the starting compound and hydrolyze its radical Z is carried out usually at a temperature in the range from room temperature to about 0 C, and preferably at a temperature in the range from 40 to C.
The reaction time is from about 1 hr to several hours.
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